Free PDF Introduction to X-Ray Powder Diffractometry
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Introduction to X-Ray Powder Diffractometry
Free PDF Introduction to X-Ray Powder Diffractometry
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From the Publisher
Illustrated with a significant amount of useful figures and diagrams this volume contains all of the fundamentals required to understand the theory and practice of powder diffraction with a strong emphasis on the two most important applications: qualitative and quantitative analysis.
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From the Inside Flap
When bombarded with X-rays, solid materials produce distinct scattering patterns similar to fingerprints. X-ray powder diffraction is a technique used to fingerprint solid samples, which are then identified and cataloged for future use-much the way the FBI keeps fingerprints on file. The current database of some 70,000 material prints has been put to a broad range of uses, from the analysis of moon rocks to testing drugs for purity. Introduction to X-ray Powder Diffractometry fully updates the achievements in the field over the past fifteen years and provides a much-needed explanation of the state-of-the-art techniques involved in characterizing materials. It covers the latest instruments and methods, with an emphasis on the fundamentals of the diffractometer, its components, alignment, calibration, and automation. The first three chapters outline diffraction theory in clear language, accessible to both students and professionals in chemistry, physics, geology, and materials science. The book's middle chapters describe the instrumentation and procedures used in X-ray diffraction, including X-ray sources, X-ray detection, and production of monochromatic radiation. The chapter devoted to instrument design and calibration is followed by an examination of specimen preparation methods, data collection, and reduction. The final two chapters provide in-depth discussions of qualitative and quantitative analysis. While the material is presented in an orderly progression, beginning with basic concepts and moving on to more complex material, each chapter stands on its own and can be studied independently or used as a professional reference. More than 230 illustrations and tables demonstrate techniques and clarify complex material. Self-contained, timely, and user-friendly, Introduction to X-ray Powder Diffractometry is an enormously useful text and professional reference for analytical chemists, physicists, geologists and materials scientists, and upper-level undergraduate and graduate students in materials science and analytical chemistry.
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Product details
Hardcover: 432 pages
Publisher: Wiley-Interscience; 1 edition (June 28, 1996)
Language: English
ISBN-10: 0471513393
ISBN-13: 978-0471513391
Product Dimensions:
6.3 x 1 x 9.2 inches
Shipping Weight: 1.5 pounds (View shipping rates and policies)
Average Customer Review:
5.0 out of 5 stars
2 customer reviews
Amazon Best Sellers Rank:
#1,592,759 in Books (See Top 100 in Books)
This book provides an introduction to powder diffraction theory as well as a comprehensive list of everything involved with the actual diffractometer. This is not just a theory book nor a technical manual. It describes clearly all the factors involved in the production of x-rays, the workings of motors and detectors to the reasons for using divergence slits as well as the principles of phase identification and quantitative analysis. It is a great book for someone who will be using a diffractometer for the first time and will be doing the work themselves. This is not a crystallography text. It is more a handbook of practical applied powder diffraction. Well worth the money.
I would suggest reading this book if you want to learn about powder XRD technique. This book is really good...
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